Abstract
The proton and 13C magnetic resonance spectra of methyl 2,3,4,6-tetra-O-methyl-alpha and -bêta-D-glucopyranoside are completely assigned. For this purpose specific deuterium and 13C labelling, spin decoupling and spectrum simulation are employed. The NMR data are discussed and compared with those of the free monomers and the methylglucosides. A partially methylated glucose
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