Development of a 1H NMR structural-reporter-group concept for the primary structural characterisation of α-D-glucans

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Development of a 1H NMR structural-reporter-group concept for the primary structural characterisation of α-D-glucans
 
van Leeuwen, S.S.; Leeflang, B.R.; Gerwig, G.J.; Kamerling, J.P.
(2008) Carbohydrate Research, volume 343, issue 6, pp. 1114 - 1119
(Article)
Abstract
An NMR study of proton chemical shift patterns of known linear α-d-glucopyranose di- and trisaccharide structures was carried out. Chemical shift patterns for (α1→2)-, (α1→3)-, (α1→4)- and (α1→6)-linked d-glucose residues were analysed and compared to literature data. Using these data, a 1H NMR structural-reporter-group concept was formulated to function as ... read more
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Keywords: Structural-reporter-group concept, a-d-Glucan1, H NMR spectroscopy, Polysaccharide structural analysis
DOI: https://doi.org/10.1016/j.carres.2008.01.043
ISSN: 0008-6215
Publisher: Elsevier BV
(Peer reviewed)
 
 
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