Abstract
Mössbauer spectra of three series of dialkylantimony(V) compounds have been measured to study bonding and structural properties of these compounds. Trialkoxodialkyl and triacetatodialkylantimony(V) compounds have octahedral structure. The former are dimeric, containing bridging methoxo groups, the latter are monomeric, containing a bidentate acetato ligand, for which the bite angle is
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